전기 환원법에 의한 (NH₄)₂[Mo(Ⅴ)OCl_(5)] 및 (PyH)₂[Mo(Ⅳ)(SCN)_(6)]들의 합성에 관한 연구
A Study on the Synthesis of Mo(Ⅴ) and Mo(Ⅳ) Complexes by the Electro-Reduction Method
광주보건전문대학논문집 1986년 11권 1호 p.95 ~ 101
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이송주/Lee SJ
KMID : 0615219860110010095
Abstract
(NH₄)₂Mo(V)OCl_(5) and(PyH)₂ Mo(Ⅳ)(SCN)_(6) complexes, molybdenum(Ⅴ)and (Ⅳ) oxidated state are syntlietized by the electro-reduction method, which has been operated easily in using the following electric cell; C ｜ Cone HCl∥MoO₃-SN-HCl｜ Hg at applied, voltage hold constant 3 volt and the current from 1.5∼2.0 amp. with a galv-anometer, these properties and composition of complexes have been identified with an elental analysis, IR-Spectra and T. G. A.
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